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Molecular Distillation Unit

  • Molecular Distillation Unit | Short Path Distillation System | Weihao Machinery
  • Professional manufacturer of molecular distillation/short path distillation systems for heat-sensitive, high-boiling materials purification. Customized, energy-saving, global service.
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Molecular Distillation Unit /Short-Path Distillation)

 

1. Core Definition & Working Principle

Molecular distillation is a specialized vacuum separation technology that relies on differences in molecular mean free paths (not boiling point difference) for purification. It operates under ultra-high vacuum (typically ≤0.01 mbar, even down to 0.001 mbar) with an extremely short distance between the heated evaporation surface and internal condensation surface (usually 1–2 cm).

  1. Degassing & Feed: Raw material is degassed to remove dissolved gases, then fed evenly into the evaporator.

  2. Wiped Thin Film Formation: Rotating scrapers spread the material into an ultra-thin liquid film (0.1–0.5 mm) on the heated wall.

  3. Molecular Evaporation: Light molecules with longer free paths escape the liquid surface and directly reach the cold condenser to form distillate. Heavy molecules can’t reach the condenser and flow down as residue.

  4. Fraction Collection: Distillate and residue are collected separately; the system maintains continuous, closed-loop operation.


Key Structural Components

  • Main Evaporator (Wiped-Film/ Centrifugal/ Falling-Film, with built-in condenser): core module

  • Ultra-high Vacuum System (Diffusion pump+Mechanical pump): to reach 10⁻³ mbar class pressure

  • Feed/ Discharge System: precise flow control

  • Heating/Cooling Circuits: jacket heating (up to 250–350°C), refrigerant cooling

  • PLC+Touch Screen Control System: full automation, data logging


2. Technical Parameters (Industrial Standard Range)

ParameterTypical Value
Operating Vacuum≤ 0.001–0.01 mbar
Heating TemperatureUp to 250°C (lab), 300–350°C (industrial)
Residence Time10–30 seconds (minimal thermal degradation)
Evaporation Area0.1 m² (lab) to 10+ m² (full-scale plant)
Feed Rate10–100 L/h (pilot), 1–50 m³/d (industrial)
Material of Construction316L Stainless Steel, Duplex Steel, PTFE linings (corrosion resistance)
Desalination/Purification PurityUp to 99.5%+ for specialty oils, pharmaceuticals, etc.

3. Main Applications

  • Food & Nutraceuticals: Purification of fish oil (EPA/DHA), squalene, vitamin E, natural flavors, and plant essential oils.

  • Pharmaceuticals: Purification of APIs, steroids, herbal extracts, removal of solvents and heavy metals.

  • Chemical & Petrochemical: Separation of polymer additives, lubricant base oils, specialty waxes, and heat-sensitive resins.

  • Cosmetics: Refinement of jojoba oil, shea butter, and high-purity cosmetic raw materials.